2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside

Base Information

Chemical Name:2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside
CAS No.:132497-70-2
Molecular Formula:C₆₇H₁₁₄NO₁₄PSi₃
Molecular Weight:1272.87
Hs Code.:

2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside

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Chemical Property of 2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside

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Technology Process of 2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside

There total 5 articles about 2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 132497-67-7,132498-16-9
2-(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 132497-70-2,132498-19-2
2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; In dichloromethane; Ambient temperature;

Reference yield:

: 122078-75-5
2-(Trimethylsilyl)ethyl 2-deoxy-4,6-O-isopropylidene-2-<(3R)-3-<(2-trimethylsilylethoxy)methoxy>tetradecanamido>-β-D-glucopyranoside

: 132497-70-2,132498-19-2
2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride, 4-dimethylaminopyridine / CH₂Cl₂ / Ambient temperature

2: 73 percent / 80percent aq. acetic acid / 2 h / 50 °C

3: 75 percent / pyridine / Ambient temperature

4: 68 percent / 4-dimethylaminopyridine, pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

Reference yield:

: 132498-61-4
(3RS)-3-(benzyloxymethoxy)decanoic acid

: 132497-70-2,132498-19-2
2(trimethylsilyl)ethyl 3-O-<(3RS)-3-(benzyloxymethoxy)decanoyl>-6-O-tert-butyldimethylsilyl-2-deoxy-4-O-diphenylphosphono-2-<(3R)-3-<2-(trimethylsilyl)ethoxymethoxy>tetradecanamido>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride, 4-dimethylaminopyridine / CH₂Cl₂ / Ambient temperature

2: 73 percent / 80percent aq. acetic acid / 2 h / 50 °C

3: 75 percent / pyridine / Ambient temperature

4: 68 percent / 4-dimethylaminopyridine, pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;