benzo[m]tetraphene-3,4-dione

Base Information

Chemical Name:benzo[m]tetraphene-3,4-dione
CAS No.:114326-31-7
Molecular Formula:C₂₂H₁₂O₂
Molecular Weight:308.336
Hs Code.:

Synonyms:

Suppliers and Price of benzo[m]tetraphene-3,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzo[m]tetraphene-3,4-dione

Chemical Property:

Vapor Pressure:1.68E-13mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of benzo[m]tetraphene-3,4-dione

There total 7 articles about benzo[m]tetraphene-3,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 83136-32-7
3-hydroxydibenzanthracene

: 114326-31-7
dibenzanthracene-3,4-dione

Guidance literature:: With potassium dihydrogenphosphate; adogen 464; potassium nitrososulfonate; In dichloromethane; benzene; for 1h;
DOI:10.1021/jm00402a009

Reference yield:

: 83136-28-1
3-methoxydibenzanthracene

: 114326-31-7
dibenzanthracene-3,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / HBr / acetic acid / 3.5 h / Heating

2: 80 percent / (KSO₃)2NO, aq. KH₂PO₄, Adogen 464 / CH₂Cl₂; benzene / 1 h

With potassium dihydrogenphosphate; adogen 464; potassium nitrososulfonate; hydrogen bromide; In dichloromethane; acetic acid; benzene;
DOI:10.1021/jm00402a009

Reference yield:

: 114326-25-9
6-methoxy-1-naphthoic acid diethylamide

: 114326-31-7
dibenzanthracene-3,4-dione

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) sec-butyllithium, TMEDA / 2) THF, -78 deg C (3 h), room temperature, overnight;

2: p-toluenesulfonic acid / benzene / 5 h / Heating

3: 92 percent / Zn, aq. KOH / pyridine / Heating

4: 93 percent / ZnCl₂ / acetic acid / 1 h / Heating

5: 100 percent / aq. HI, aq. hypophosphorous acid / acetic acid / 0.03 h / 100 °C

6: 100 percent / HBr / acetic acid / 3.5 h / Heating

7: 80 percent / (KSO₃)2NO, aq. KH₂PO₄, Adogen 464 / CH₂Cl₂; benzene / 1 h

With potassium hydroxide; potassium dihydrogenphosphate; adogen 464; potassium nitrososulfonate; N,N,N,N,-tetramethylethylenediamine; hydrogen bromide; hydrogen iodide; sec.-butyllithium; hypophosphorous acid; toluene-4-sulfonic acid; zinc(II) chloride; zinc; In pyridine; dichloromethane; acetic acid; benzene;
DOI:10.1021/jm00402a009