Mo(η6-PhPMePh)(dptpe)(PMePh2)

Base Information

Chemical Name:Mo(η6-PhPMePh)(dptpe)(PMePh2)
CAS No.:122068-50-2
Molecular Formula:C₅₆H₅₈MoP₄
Molecular Weight:950.912
Hs Code.:

Synonyms:

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Chemical Property of Mo(η6-PhPMePh)(dptpe)(PMePh2)

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Technology Process of Mo(η6-PhPMePh)(dptpe)(PMePh2)

There total 1 articles about Mo(η6-PhPMePh)(dptpe)(PMePh2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 84430-77-3
(η6-C6H5PPhMe)Mo(PPh2Me)3

: 70320-30-8
1,2-bis[di(p-tolyl)phosphino]ethane

: 122068-50-2
Mo(η6-PhPMePh)(dptpe)(PMePh2)

Guidance literature:: In benzene; dissolving of Mo(η6-PhPMePh)(PMePh2)3 and dptpe in dry benzene under N2, refluxing of the orange-red soln. (0.5 h), removing of benzene (vac.), drying of the oil in a pistol (refluxing acetone as heat source, 8 h), stirring in dry methanol (6 h); filtration, recrystn. (toluene/methanol); elem. anal.;

Reference yield: 15.0%

: tetrafluoroboric acid

: 122068-50-2
Mo(η6-PhPMePh)(dptpe)(PMePh2)

: {Mo(O)(F)(dptpe)2}⁽¹⁺⁾

: Mo(η6-C6H6)(dptpe)(PMePhOH)(H)(1+)*BF4(1-)

Guidance literature:: In water; benzene; byproducts: HPMePh2(1+); dropwise addn. of aq. HBF4 to a soln. of the complex in water-satd. benzene (room temp.), formation of a brown oil (after 5 min) and a colorless benzene supernatant (after 10 min), removing of benzene and water; further products: unidentified species; dry-pumping of the residue, redissolving in acetone;

Reference yield:

: tetrafluoroboric acid

: 122068-50-2
Mo(η6-PhPMePh)(dptpe)(PMePh2)

: 98703-44-7
Mo(η6-PhPPh2)(dppe)(PPh3)

: Mo(η6-C6H6)(dptpe)(PMePhOH)(H)(1+)*BF4(1-)

: Mo(η6-C6H6)(dppe)(PPh2OH)(H)(1+)*BF4(1-)

: Mo(η6-C6H6)(dppe)(PMePhOH)(H)(1+)*BF4(1-)

: Mo(η6-C6H6)(dptpe)(PPh2OH)(H)(1+)*BF4(1-)

Guidance literature:: In water; benzene; dissolving of both complexes in water-satd. benzene, dropwise addn. of aq. HBF4 (vigorous stirring); not isolated; detn. by 31P-NMR;