C₆₀H₇₇NO₁₆Si₂

Base Information

Chemical Name:C₆₀H₇₇NO₁₆Si₂
CAS No.:253327-76-3
Molecular Formula:C₆₀H₇₇NO₁₆Si₂
Molecular Weight:1124.44
Hs Code.:

C<sub>60</sub>H<sub>77</sub>NO<sub>16</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₆₀H₇₇NO₁₆Si₂

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Technology Process of C₆₀H₇₇NO₁₆Si₂

There total 19 articles about C₆₀H₇₇NO₁₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 253327-75-2
C₆₀H₇₉NO₁₇Si₂

: 253327-76-3
C₆₀H₇₇NO₁₆Si₂

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0960-894X(99)00522-3

Reference yield:

: 626-18-6
1,3-dimethanol benzene

: 253327-76-3
C₆₀H₇₇NO₁₆Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: 68 percent / PCC / CH₂Cl₂

2: 82 percent / Et₃N / CH₂Cl₂

3: 100 percent / tetrahydrofuran

4: tetrahydrofuran / -78 - 20 °C

5: 88 percent / 0.25 percent aq. HCl / methanol

6: PDC

7: KMnO₄

8: 90 percent / DCC; DMAP / toluene

9: 75 percent / Et₃N / CH₂Cl₂

10: 15 percent / NaHMDS / tetrahydrofuran / -78 - 20 °C

11: 100 percent / H₂ / Pd/C / tetrahydrofuran

12: 21 percent / BOP-Cl; Et₃N / CH₂Cl₂

With hydrogenchloride; dmap; potassium permanganate; dipyridinium dichromate; hydrogen; sodium hexamethyldisilazane; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; dicyclohexyl-carbodiimide; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene; 1: Oxidation / 2: silylation / 3: amidosilylation / 4: asymmetric cyclocondensation / 5: Hydrolysis / 6: Oxidation / 7: Oxidation / 8: Esterification / 9: Acylation / 10: Condensation / 11: Hydrogenolysis / 12: macrolactonization;
DOI:10.1016/S0960-894X(99)00522-3

Reference yield:

: 994-30-9
triethylsilyl chloride

: 253327-76-3
C₆₀H₇₇NO₁₆Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / pyridine

2: 15 percent / NaHMDS / tetrahydrofuran / -78 - 20 °C

3: 100 percent / H₂ / Pd/C / tetrahydrofuran

4: 21 percent / BOP-Cl; Et₃N / CH₂Cl₂

With pyridine; hydrogen; sodium hexamethyldisilazane; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; 1: silylation / 2: Condensation / 3: Hydrogenolysis / 4: macrolactonization;
DOI:10.1016/S0960-894X(99)00522-3