triphenylgermyltetracarbonylcobalt

Base Information

Chemical Name:triphenylgermyltetracarbonylcobalt
CAS No.:64023-44-5
Molecular Formula:C₂₂H₁₅CoGeO₄
Molecular Weight:474.942
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylgermyltetracarbonylcobalt

Chemical Property:

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Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of triphenylgermyltetracarbonylcobalt

There total 1 articles about triphenylgermyltetracarbonylcobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14971-27-8,71564-35-7
cobalt tetracarbonyl anion

: 3005-32-1
triphenylgermanium bromide

: 64023-44-5,16560-95-5,30406-47-4
Ph₃GeCo(CO)4

Guidance literature:: In tetrahydrofuran; methanol; on treatment of soln. of (Co(CO)4)(1-) in methanol at 40°C for 10min with soln. of (C6H5)3GeBr in THF;; on pptg. from cooled soln. with H2O; recrystg. from pentane;;

Reference yield: 82.0%

: 64023-44-5,16560-95-5,30406-47-4
Ph₃GeCo(CO)4

: 7781-71-7
tetraethylammonium trichloro-stannate(II)

: 1626-24-0
chlorotriphenylgermane

Guidance literature:: In tetrahydrofuran; under N2 to a soln. of Co-complex in THF was added a THF soln. of Et4NSnCl3 at room temp., stirred for 3 d; filtered, pumped off, extd. with n-pentane, pumped off;
DOI:10.1016/S0022-328X(00)82934-4

Reference yield: 74.0%

: 16853-85-3
lithium aluminium tetrahydride

: 64023-44-5,16560-95-5,30406-47-4
Ph₃GeCo(CO)4

: 2816-43-5
triphenylgermane

Guidance literature:: With hydrogenchloride; In diethyl ether; under N2 a soln. of Co-complex in ether was stirred for 2 d at room temp. with excess of LiAlH4, hydrolysis with aq. HCl; chromd. (silica gel, hexane/benzene);
DOI:10.1016/S0022-328X(00)82934-4