Technology Process of C30H36F2O11
There total 12 articles about C30H36F2O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(bis-(2-methoxyethyl)amino)sulfur trufluoride;
In
chloroform;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ol200808q
- Guidance literature:
-
C30H36O12;
With
(bis-(2-methoxyethyl)amino)sulfur trufluoride;
In
chloroform;
at 0 - 20 ℃;
Inert atmosphere;
With
sodium tetrahydroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
ethanol;
at 0 - 50 ℃;
DOI:10.1021/ol200808q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / acetonitrile / 0 - 20 °C / Inert atmosphere
2: dmap / dichloromethane / 0 - 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 20 °C
4: [bis(acetoxy)iodo]benzene; magnesium oxide / chloroform / 0 - 20 °C
5: (bis-(2-methoxyethyl)amino)sulfur trufluoride / chloroform / 0 - 20 °C / Inert atmosphere
With
dmap; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; magnesium oxide; acetic acid; triethylamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride;
In
tetrahydrofuran; dichloromethane; chloroform; acetonitrile;
DOI:10.1021/ol200808q