5-[4-(dibutoxyphosphorylamino)]phenyl-10,15,20-triphenylporphyrinato gold(III) chloride

Base Information

• Chemical Name: 5-[4-(dibutoxyphosphorylamino)]phenyl-10,15,20-triphenylporphyrinato gold(III) chloride
• CAS No.: 1408288-30-1
• Molecular Formula: C₅₂H₄₆AuN₅O₃P*Cl
• Molecular Weight: 1052.36
• Mol file: 1408288-30-1.mol

Synonyms:

Chemical Property of 5-[4-(dibutoxyphosphorylamino)]phenyl-10,15,20-triphenylporphyrinato gold(III) chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-[4-(dibutoxyphosphorylamino)]phenyl-10,15,20-triphenylporphyrinato gold(III) chloride

There total 2 articles about 5-[4-(dibutoxyphosphorylamino)]phenyl-10,15,20-triphenylporphyrinato gold(III) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.2%

potassium tetrachloroaurate(III) (13682-61-6) + 5-[4-(dibutoxyphosphorylamino)phenyl]-10,15,20-triphenylporphyrin → 5-[4-(dibutoxyphosphorylamino)]phenyl-10,15,20-triphenylporphyrinato gold(III) chloride (1408288-30-1)

Guidance literature:

With sodium acetate; In acetic acid; for 18h; Reflux;

DOI:10.3184/174751912X13406179445757

Reference yield:

5-(4-nitrophenyl)-10,15,20-triphenylporphyrin (67605-65-6) → 5-[4-(dibutoxyphosphorylamino)]phenyl-10,15,20-triphenylporphyrinato gold(III) chloride (1408288-30-1)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride; tin(ll) chloride / water / 1 h / 0 °C / Inert atmosphere

2: tetrachloromethane; triethylamine; 1,4-dioxane / 3 h / 25 °C

3: sodium acetate / acetic acid / 18 h / Reflux

With hydrogenchloride; sodium acetate; tin(ll) chloride; In 1,4-dioxane; tetrachloromethane; water; acetic acid; triethylamine;

DOI:10.3184/174751912X13406179445757

upstream raw materials:

potassium tetrachloroaurate(III)

5-(4-nitrophenyl)-10,15,20-triphenylporphyrin