Technology Process of C11H12BrNO3S
There total 4 articles about C11H12BrNO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(2-carboxyethyl)-phosphine hydrochloride;
In
water; dimethyl sulfoxide;
at 25 ℃;
for 0.333333h;
Darkness;
DOI:10.1021/jm2016182
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; water / Reflux
2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C
3: tris-(2-carboxyethyl)-phosphine hydrochloride / water; dimethyl sulfoxide / 0.33 h / 25 °C / Darkness
With
hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; tris-(2-carboxyethyl)-phosphine hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/jm2016182
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium acetate / Reflux
2: hydrogenchloride; water / Reflux
3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C
4: tris-(2-carboxyethyl)-phosphine hydrochloride / water; dimethyl sulfoxide / 0.33 h / 25 °C / Darkness
With
hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; sodium acetate; tris-(2-carboxyethyl)-phosphine hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/jm2016182