[AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)(benzyloxy)(THF)2]

Base Information

Chemical Name:[AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)(benzyloxy)(THF)2]
CAS No.:1333519-48-4
Molecular Formula:C₆₀H₈₉AlNNaO₆
Molecular Weight:970.341
Hs Code.:

Synonyms:

Suppliers and Price of [AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)(benzyloxy)(THF)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)(benzyloxy)(THF)2]

Chemical Property:

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Technology Process of [AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)(benzyloxy)(THF)2]

There total 2 articles about [AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)(benzyloxy)(THF)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1333519-47-3
[AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)Me(THF)2]

: 100-51-6,185532-71-2
benzyl alcohol

: 1333519-48-4
[AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)(benzyloxy)(THF)2]

Guidance literature:: In toluene; PhCH2OH in toluene added to stirred soln. of Al complex in toluene at 50°C; stirred for 12 h; solvent removed under vac.; dissolved in THF-hexane; filtered through Celite; crystd. from filtrate at room temp. for several d; elem. anal.;
DOI:10.1021/ic2013123

Reference yield: 52.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 350484-86-5
tris(4,6-di-tert-butyl-2-hydroxybenzyl)amine

: 75-24-1
trimethylaluminum

: 7440-23-5
sodium

: 100-51-6,185532-71-2
benzyl alcohol

: 1333519-48-4
[AlNa(tris(2-oxy-4,6-di-tert-butyl-benzyl)amine)(benzyloxy)(THF)2]

Guidance literature:: In toluene; under N2; soln. of ligand and Na (molar ratio 1:2.2) stirred in THF at 50°C until Na dissolved completely; AlMe3 in hexane slowly added; stirred (12 h); solvent removed under vac.; dissolved in toluene; PhCH2OH in toluene added; stirred for 24 h; solvent removed under vac.; dissolved in THF-hexane; filtered through Celite; crystd. from filtrate at room temp. for several d; elem. anal.;
DOI:10.1021/ic2013123