C₁₇H₁₄N₄O₂

Base Information

Chemical Name:C₁₇H₁₄N₄O₂
CAS No.:1380230-80-7
Molecular Formula:C₁₇H₁₄N₄O₂
Molecular Weight:306.324
Hs Code.:

C<sub>17</sub>H<sub>14</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₄N₄O₂

Chemical Property:

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Technology Process of C₁₇H₁₄N₄O₂

There total 4 articles about C₁₇H₁₄N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1380230-80-7
C₁₇H₁₄N₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -20 °C / Inert atmosphere

1.2: 0.33 h / -20 °C / Inert atmosphere

2.1: trifluoroacetic acid / 0.5 h

3.1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 20 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; isobutyl chloroformate; In tetrahydrofuran; methanol; trifluoroacetic acid; 4.1: Mitsunobu reaction;
DOI:10.1021/ol3012106

Reference yield:

: 3182-95-4
L-Phenylalaninol

: 1380230-80-7
C₁₇H₁₄N₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; 2: Mitsunobu reaction;
DOI:10.1021/ol3012106

Reference yield:

: 66605-57-0
(S)-N-tert-butoxycarbonyl-2-amino-3-phenylpropanol

: 1380230-80-7
C₁₇H₁₄N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / 0.5 h

2: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 20 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; trifluoroacetic acid; 3: Mitsunobu reaction;
DOI:10.1021/ol3012106