Re2Br4(μ-Ph2PCH2PPh2)2(xylyl isocyanide)

Base Information

Chemical Name:Re2Br4(μ-Ph2PCH2PPh2)2(xylyl isocyanide)
CAS No.:106855-95-2
Molecular Formula:C₅₉H₅₃Br₄NP₄Re₂
Molecular Weight:1592
Hs Code.:

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Chemical Property of Re2Br4(μ-Ph2PCH2PPh2)2(xylyl isocyanide)

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Technology Process of Re2Br4(μ-Ph2PCH2PPh2)2(xylyl isocyanide)

There total 1 articles about Re2Br4(μ-Ph2PCH2PPh2)2(xylyl isocyanide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 58312-72-4
Re₂Br₄(dppm)2

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 106855-95-2
Re2Br4(μ-Ph2PCH2PPh2)2(xylyl isocyanide)

Guidance literature:: In toluene; under nitrogen; dropwise addn. of isocyanide to complex soln., mixt. stirred for 5 min; pptd. (diethyl ether); filtered; washed (diethyl ether); dried (vac.); elem. anal.;
DOI:10.1039/DT9860002607

Reference yield: 73.0%

: 106855-95-2
Re2Br4(μ-Ph2PCH2PPh2)2(xylyl isocyanide)

: 7726-95-6
bromine

: [Re2Br5(μ-Ph2PCH2PPh2)2(xylyl isocyanide)]Br3

Guidance literature:: In dichloromethane; 1,2-dichloro-ethane; under N2; Re-complex in CH2Cl2 treated with soln. of Br2 in 1,2-dichloroethane, stirred for 10 min; reduced in vol., Et2O added, crystn. on cooling to 0°C; elem. anal.;
DOI:10.1016/S0022-328X(99)00535-5