bis(1,3-bis(4-decyloxyphenyl)-imidazol-1-ium)palladium(II) diiodide

Base Information

• Chemical Name: bis(1,3-bis(4-decyloxyphenyl)-imidazol-1-ium)palladium(II) diiodide
• CAS No.: 1050282-73-9
• Molecular Formula: C₇₀H₁₀₄I₂N₄O₄Pd
• Molecular Weight: 1425.85
• Mol file: 1050282-73-9.mol

Synonyms:

Chemical Property of bis(1,3-bis(4-decyloxyphenyl)-imidazol-1-ium)palladium(II) diiodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of bis(1,3-bis(4-decyloxyphenyl)-imidazol-1-ium)palladium(II) diiodide

There total 1 articles about bis(1,3-bis(4-decyloxyphenyl)-imidazol-1-ium)palladium(II) diiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

1,3-bis(4-decyloxyphenyl)-3H-imidazol-1-ium trifluoromethanesulfonate (1050282-65-9) + palladium diacetate (3375-31-3) + sodium iodide (7681-82-5,24359-64-6,41927-88-2,115813-40-6) → bis(1,3-bis(4-decyloxyphenyl)-imidazol-1-ium)palladium(II) diiodide (1050282-73-9)

Guidance literature:

With tBuOK; In tetrahydrofuran; (N2), ligand , Pd(OAc)2 and NaI (2:1:2) suspnd. in THF, treated with 2 equiv. of tBuOK, stirred at 40°C for 1.5 d; evapd., extd.(CH2Cl2/H2O), DCM layer dried (Na2SO4), evapd., chromy.(SiO2 - CH2Cl2/pentane), elem. anal.;

DOI:10.1002/ejic.200700251

upstream raw materials:

1,3-bis(4-decyloxyphenyl)-3H-imidazol-1-ium trifluoromethanesulfonate

palladium diacetate

sodium iodide