Technology Process of C28H25N3O3
There total 4 articles about C28H25N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
dichloromethane; dimethyl sulfoxide;
for 96h;
Inert atmosphere;
Schlenk technique;
Reflux;
DOI:10.1039/c3dt50850a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dichloromethane / 7 h / 20 °C / Inert atmosphere
2: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine / N,N-dimethyl-formamide / 96 h / 75 °C / Inert atmosphere; Schlenk technique
3: potassium carbonate / dichloromethane; dimethyl sulfoxide / 96 h / Inert atmosphere; Schlenk technique; Reflux
With
copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate; triethylamine;
In
dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c3dt50850a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: n-butyllithium / diethyl ether / -78 °C
2: dichloromethane / 7 h / 20 °C / Inert atmosphere
3: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine / N,N-dimethyl-formamide / 96 h / 75 °C / Inert atmosphere; Schlenk technique
4: potassium carbonate / dichloromethane; dimethyl sulfoxide / 96 h / Inert atmosphere; Schlenk technique; Reflux
With
copper(l) iodide; n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate; triethylamine;
In
diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c3dt50850a
