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trans-bis(glycinato)nickel(II)

Base Information
  • Chemical Name:trans-bis(glycinato)nickel(II)
  • CAS No.:14215-37-3
  • Molecular Formula:C4H8N2NiO4
  • Molecular Weight:206.809
  • Hs Code.:
trans-bis(glycinato)nickel(II)

Synonyms:

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Chemical Property of trans-bis(glycinato)nickel(II)
Chemical Property:
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Technology Process of trans-bis(glycinato)nickel(II)

There total 3 articles about trans-bis(glycinato)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With KOH; In water; mixing of 2 equiv. of glycine and 1 equiv. of Ni(NO3)2; heating to 70°C for 2 h; dissolving in H2O under stirring and heating for 1 h; adjusting pH to 6.0 by addn. of KOH; standing for 4 ds; concn. under constant stirring; cooling to 4°C; slow pptn., purification with H2O, EtOH and HNO3; sepn., drying and storage in desiccators with CaCl2; elem. anal.;
DOI:10.1016/j.saa.2006.11.055
Guidance literature:
In neat (no solvent, solid phase); dried at 150°C in vac. oven;
DOI:10.1246/bcsj.57.2622
Guidance literature:
In water; dissolving freshly pptd. NiCO3 in an aq. glycine soln.; recrystn. from water;
DOI:10.1246/bcsj.59.1487
upstream raw materials:

nickel(II) carbonate

glycine

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