C₂₇H₃₂N₄O₉S

Base Information

Chemical Name:C₂₇H₃₂N₄O₉S
CAS No.:1298088-63-7
Molecular Formula:C₂₇H₃₂N₄O₉S
Molecular Weight:588.638
Hs Code.:

C<sub>27</sub>H<sub>32</sub>N<sub>4</sub>O<sub>9</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₂N₄O₉S

Chemical Property:

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Technology Process of C₂₇H₃₂N₄O₉S

There total 6 articles about C₂₇H₃₂N₄O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 1232149-67-5
H-Gly-L-Cys(S-Z-L-Ala)-OH

: 1232149-54-0
Z-L-Ala-Gly-L-Cys-OH

: 1298088-63-7
C₂₇H₃₂N₄O₉S

Guidance literature:: In acetonitrile; at 50 ℃; for 1h; pH=7.8; Microwave irradiation; aq. phosphate buffer; Inert atmosphere;
DOI:10.1039/c003234d

Reference yield:

: Fmoc-Glu-Cys

: 1298088-63-7
C₂₇H₃₂N₄O₉S

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydrogencarbonate / water; acetonitrile / 0.5 h / 10 - 20 °C

1.2: 20 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

2.2: Inert atmosphere

2.3: pH 5 / Inert atmosphere

3.1: water; acetonitrile / 1 h / 50 - 70 °C / pH 7.8 / aq. phosphate buffer; Inert atmosphere; Microwave irradiation

With potassium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/jo1015757

Reference yield:

: 1232149-64-2
N-Fmoc-Gly-L-Cys(S-Z-L-Ala)-OH

: 1298088-63-7
C₂₇H₃₂N₄O₉S

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere

1.3: pH 5 / Inert atmosphere

2.1: water; acetonitrile / 1 h / 50 - 70 °C / pH 7.8 / aq. phosphate buffer; Inert atmosphere; Microwave irradiation

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/jo1015757