Technology Process of C46H54N2O8S
There total 5 articles about C46H54N2O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1.5 h / 20 °C
2: triethylamine / dichloromethane / 0.5 h / 20 °C
With
sodium tris(acetoxy)borohydride; triethylamine;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/chem.201200376
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: 3 h / -78 °C / Inert atmosphere
2.1: copper(l) cyanide; 4-penten-1-ylmagnesium bromide / tetrahydrofuran / 1 h / -78 °C
2.2: 1 h / -78 °C
3.1: dmap; pyridine; phenylcarbonochloridothioate / 12 h / 20 °C
3.2: 1 h / 80 °C
4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile; water / 4 h / 20 °C
5.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1.5 h / 20 °C
6.1: triethylamine / dichloromethane / 0.5 h / 20 °C
With
pyridine; dmap; copper(l) cyanide; 4-penten-1-ylmagnesium bromide; sodium tris(acetoxy)borohydride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; phenylcarbonochloridothioate; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1002/chem.201200376
