C₂₉H₂₈FN₅O

Base Information

Chemical Name:C₂₉H₂₈FN₅O
CAS No.:1421502-75-1
Molecular Formula:C₂₉H₂₈FN₅O
Molecular Weight:481.573
Hs Code.:

C<sub>29</sub>H<sub>28</sub>FN<sub>5</sub>O

Synonyms:

Suppliers and Price of C₂₉H₂₈FN₅O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₉H₂₈FN₅O

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₉H₂₈FN₅O

There total 14 articles about C₂₉H₂₈FN₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421503-45-8
1-bromo-2-ethyl-5-fluoro-4-methoxy-benzene

: 1421502-75-1
C₂₉H₂₈FN₅O

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylamine; dichloro bis(acetonitrile) palladium(II); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 18 h / 110 °C / Inert atmosphere

2.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 18 h / 110 °C / Inert atmosphere

3.1: hydrogenchloride; water / methanol / 60 °C

4.1: potassium hydroxide / N,N-dimethyl-formamide / 0.08 h

4.2: 0.5 h / 20 °C

5.1: toluene-4-sulfonic acid / dichloromethane / 0 - 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 18 h / 100 °C / Inert atmosphere

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / toluene / 18 h / 100 °C / Inert atmosphere

8.1: hydrogenchloride; water / methanol / 36 h / 60 °C

9.1: boron tribromide / dichloromethane / 18 h / 0 - 20 °C

10.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 50 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; dichloro bis(acetonitrile) palladium(II); potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; boron tribromide; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1421503-46-9
2-(2-ethyl-5-fluoro-4-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1421502-75-1
C₂₉H₂₈FN₅O

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 18 h / 110 °C / Inert atmosphere

2.1: hydrogenchloride; water / methanol / 60 °C

3.1: potassium hydroxide / N,N-dimethyl-formamide / 0.08 h

3.2: 0.5 h / 20 °C

4.1: toluene-4-sulfonic acid / dichloromethane / 0 - 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 18 h / 100 °C / Inert atmosphere

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / toluene / 18 h / 100 °C / Inert atmosphere

7.1: hydrogenchloride; water / methanol / 36 h / 60 °C

8.1: boron tribromide / dichloromethane / 18 h / 0 - 20 °C

9.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 50 °C

With hydrogenchloride; potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; boron tribromide; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1234845-77-2
4-ethyl-1-fluoro-2-methoxy-benzene

: 1421502-75-1
C₂₉H₂₈FN₅O

Guidance literature:: Multi-step reaction with 11 steps

1.1: N-Bromosuccinimide / acetonitrile / 18 h / 20 °C

2.1: triethylamine; dichloro bis(acetonitrile) palladium(II); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane / 18 h / 110 °C / Inert atmosphere

3.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 18 h / 110 °C / Inert atmosphere

4.1: hydrogenchloride; water / methanol / 60 °C

5.1: potassium hydroxide / N,N-dimethyl-formamide / 0.08 h

5.2: 0.5 h / 20 °C

6.1: toluene-4-sulfonic acid / dichloromethane / 0 - 20 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 18 h / 100 °C / Inert atmosphere

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / toluene / 18 h / 100 °C / Inert atmosphere

9.1: hydrogenchloride; water / methanol / 36 h / 60 °C

10.1: boron tribromide / dichloromethane / 18 h / 0 - 20 °C

11.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 50 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; dichloro bis(acetonitrile) palladium(II); potassium phosphate; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; boron tribromide; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;