C₂₄H₂₇N₃O₃S

Base Information

Chemical Name:C₂₄H₂₇N₃O₃S
CAS No.:1392139-46-6
Molecular Formula:C₂₄H₂₇N₃O₃S
Molecular Weight:437.563
Hs Code.:

C<sub>24</sub>H<sub>27</sub>N<sub>3</sub>O<sub>3</sub>S

Synonyms:

Suppliers and Price of C₂₄H₂₇N₃O₃S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₄H₂₇N₃O₃S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₄H₂₇N₃O₃S

There total 4 articles about C₂₄H₂₇N₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 26116-12-1
1-ethyl-2-pyrrolidinemethanamine

: 1392139-28-4
(Z)-2-(2-methoxybenzylidene)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]thiazine-6-carboxylic acid

: 1392139-46-6
C₂₄H₂₇N₃O₃S

Guidance literature:: (Z)-2-(2-methoxybenzylidene)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]thiazine-6-carboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 23 ℃; for 0.0833333h;

1-ethyl-2-pyrrolidinemethanamine; In dichloromethane; for 15h;
DOI:10.1021/jm300833h

Reference yield:

: 453-71-4
3-nitro-4-fluorobenzoic acid

: 1392139-46-6
C₂₄H₂₇N₃O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / 15 h / Reflux

2.1: triethylamine / acetonitrile / 15 h / 85 °C

3.1: iron; acetic acid / acetonitrile / 1 h / 0 - 80 °C

4.1: acetic anhydride; triethylamine / 15 h / Reflux

5.1: lithium hydroxide / methanol; water / 15 h / 23 °C

6.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 23 °C

6.2: 15 h

With sulfuric acid; acetic anhydride; iron; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jm300833h

Reference yield:

: 204863-53-6
ethyl 3-oxo-3,4-dihydro-2H-benzo[b][1,4]thiazine-6-carboxylate

: 1392139-46-6
C₂₄H₂₇N₃O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride; triethylamine / 15 h / Reflux

2.1: lithium hydroxide / methanol; water / 15 h / 23 °C

3.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 23 °C

3.2: 15 h

With acetic anhydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In methanol; dichloromethane; water;
DOI:10.1021/jm300833h