C₅₄H₆₉N₇O₁₁S

Base Information

Chemical Name:C₅₄H₆₉N₇O₁₁S
CAS No.:1415033-94-1
Molecular Formula:C₅₄H₆₉N₇O₁₁S
Molecular Weight:1024.25
Hs Code.:

C<sub>54</sub>H<sub>69</sub>N<sub>7</sub>O<sub>11</sub>S

Synonyms:

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Chemical Property of C₅₄H₆₉N₇O₁₁S

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Technology Process of C₅₄H₆₉N₇O₁₁S

There total 11 articles about C₅₄H₆₉N₇O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₈N₄O₅

: 1415034-18-2
C₂₉H₃₃N₃O₇S

: 1415033-94-1
C₅₄H₆₉N₇O₁₁S

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jm301630s

Reference yield:

: 695215-94-2
3-(methoxycarbonyl)-5-[methyl(methylsulfonyl)amino]benzoic acid

: 1415033-94-1
C₅₄H₆₉N₇O₁₁S

Guidance literature:: Multi-step reaction with 5 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C / Cooling with ice

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

5: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0 - 20 °C

With 1-hydroxy-7-aza-benzotriazole; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm301630s

Reference yield:

: 695215-93-1
dimethyl-5-[methyl(methylsulfonyl)amino]isophthalate

: 1415033-94-1
C₅₄H₆₉N₇O₁₁S

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / tetrahydrofuran; methanol; water / 0 - 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

3: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C / Cooling with ice

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

5: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

6: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0 - 20 °C

With 1-hydroxy-7-aza-benzotriazole; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/jm301630s