[Mg(C₄H₈O)6]⁽²⁺⁾*[Cr(C₆F₅)4]^(2-)=[Mg(C₄H₈O)6][Cr(C₆F₅)4]

Base Information

Chemical Name:[Mg(C₄H₈O)6]⁽²⁺⁾*[Cr(C₆F₅)4]^(2-)=[Mg(C₄H₈O)6][Cr(C₆F₅)4]
CAS No.:858346-92-6
Molecular Formula:C₂₄CrF₂₀*C₂₄H₄₈MgO₆
Molecular Weight:1177.17
Hs Code.:

[Mg(C<sub>4</sub>H<sub>8</sub>O)6]<sup>(2+)</sup>*[Cr(C<sub>6</sub>F<sub>5</sub>)4]<sup>(2-)</sup>=[Mg(C<sub>4</sub>H<sub>8</sub>O)6][Cr(C<sub>6</sub>F<sub>5</sub>)4]

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Chemical Property of [Mg(C₄H₈O)6]⁽²⁺⁾*[Cr(C₆F₅)4]^(2-)=[Mg(C₄H₈O)6][Cr(C₆F₅)4]

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Technology Process of [Mg(C₄H₈O)6]⁽²⁺⁾*[Cr(C₆F₅)4]^(2-)=[Mg(C₄H₈O)6][Cr(C₆F₅)4]

There total 1 articles about [Mg(C₄H₈O)6]⁽²⁺⁾*[Cr(C₆F₅)4]^(2-)=[Mg(C₄H₈O)6][Cr(C₆F₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 36463-97-5
CrCl₂(THF)

: 879-05-0
2,3,4,5,6-pentafluorophenylmagnesium bromide

: 858346-92-6
[Mg(C₄H₈O)6]⁽²⁺⁾*[Cr(C₆F₅)4]^(2-)=[Mg(C₄H₈O)6][Cr(C₆F₅)4]

Guidance literature:: In tetrahydrofuran; diethyl ether; under Ar, Schlenk technique; suspn. of Cr compd. in THF slowly added to soln. of Mg compd. in Et2O at -78°C; mixt. allowed to warm to 0°C and stirred at this temp. for 3 h; 1,4-dioxane added; stored at -30°C for 2 d; white ppt. removed byfiltration; filtrate evapd. under vac.; elem. anal.;
DOI:10.1021/om050206e