tris(pentachlorophenyl)gold(III) tetrahydrothiophen complex

Base Information

• Chemical Name: tris(pentachlorophenyl)gold(III) tetrahydrothiophen complex
• CAS No.: 110544-42-8
• Molecular Formula: C₂₂H₈AuCl₁₅S
• Molecular Weight: 1033.13

Synonyms:

Chemical Property of tris(pentachlorophenyl)gold(III) tetrahydrothiophen complex

Chemical Property:

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Technology Process of tris(pentachlorophenyl)gold(III) tetrahydrothiophen complex

There total 1 articles about tris(pentachlorophenyl)gold(III) tetrahydrothiophen complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

Au(I)(C6Cl5)(tetrahydrothiophene) + Tl(3+)*2C6Cl5(1-)*Cl(1-)=Tl(C6Cl5)2Cl → tris(pentachlorophenyl)gold(III) tetrahydrothiophen complex (110544-42-8)

Guidance literature:

In toluene; byproducts: TlCl; Tl(C6Cl5)2Cl added to a soln. of the Au compd. in toluene, mixt. refluxed for 2 h; filtered, filtrate evapd. to dryness, recrystd. from Et2O-hexane; elem.anal.;

DOI:10.1016/S0020-1693(00)81271-2

Reference yield: 78.0%

tris(pentachlorophenyl)gold(III) tetrahydrothiophen complex (110544-42-8) + Methyltriphenylphosphonium bromide (1779-49-3) → CH3P(C6H5)3(1+)*Au(C6Cl5)3Br(1-)=[CH3P(C6H5)3][Au(C6Cl5)3Br] (110544-49-5)

Guidance literature:

In dichloromethane; (PPh3Me)Br added to a soln. of the Au compd. in CH2Cl2, mixt. stirred at room temp. for 1 h; soln. evapd., hexane added, pptn.; elem. anal.;

DOI:10.1016/S0020-1693(00)81271-2

Reference yield: 75.0%

tris(pentachlorophenyl)gold(III) tetrahydrothiophen complex (110544-42-8) + dimethyldiphenylphosphonium iodide (1017-88-5) → (CH3)2P(C6H5)2(1+)*Au(C6Cl5)3I(1-)=[(CH3)2P(C6H5)2][Au(C6Cl5)3I] (110566-80-8)

Guidance literature:

In dichloromethane; (PPh2Me2)I added to a soln. of the Au compd. in CH2Cl2, mixt. stirred at room temp. for 1 h; soln. evapd., hexane added, pptn.; elem. anal.;

DOI:10.1016/S0020-1693(00)81271-2

Downstream raw materials:

(CH₃)2P(C₆H₅)2⁽¹⁺⁾*Au(C₆Cl₅)3I^(1-)=[(CH₃)2P(C₆H₅)2][Au(C₆Cl₅)3I]

N(P(C₆H₅)3)2⁽¹⁺⁾*Au(C₆Cl₅)3Cl^(1-)=[N(P(C₆H₅)3)2][Au(C₆Cl₅)3Cl]

tris(pentachlorophenyl)gold(III) bis(diphenylphosphino)methane complex

CH₃P(C₆H₅)3⁽¹⁺⁾*Au(C₆Cl₅)3Br^(1-)=[CH₃P(C₆H₅)3][Au(C₆Cl₅)3Br]

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