β-pyridinium zinc tetraphenylporphyrin chloride

Base Information

Chemical Name:β-pyridinium zinc tetraphenylporphyrin chloride
CAS No.:105821-47-4
Molecular Formula:C₄₉H₃₂N₅Zn*Cl
Molecular Weight:791.67
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Chemical Property of β-pyridinium zinc tetraphenylporphyrin chloride

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Technology Process of β-pyridinium zinc tetraphenylporphyrin chloride

There total 1 articles about β-pyridinium zinc tetraphenylporphyrin chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 14074-80-7
zinc tetraphenylporphyrin

: 71435-57-9
(2-nitro-5,10,15,20-tetraphenylporphyrinato)zinc(II)

: 105821-47-4
β-pyridinium zinc tetraphenylporphyrin chloride

Guidance literature:: With pyridine; nitronium tetrafluoborate; In pyridine; stirring a solution of zinc(II) meso-tetraphenylporphyrin (178 mg) in pyridine (10 ml) with nitronium tetrafluoroborate (347 mg), partitioning between water (100 ml) and chloroform (100 ml), washing with water and evaporation;; chromatography (toluene, alumina Grade III); first (minor) fraction 5 mg unreacted Zn porhpyrin and traces of β-nitro-Zn meso-tetraphenyl porphyrin; second (main) fraction was recrystd. from CH2Cl2-hexane;;