12-{2-[bis(but-2-ynyl)amino]phenoxy}dodecanenitrile

Base Information

• Chemical Name: 12-{2-[bis(but-2-ynyl)amino]phenoxy}dodecanenitrile
• CAS No.: 1365564-03-9
• Molecular Formula: C₂₆H₃₆N₂O
• Molecular Weight: 392.585

Synonyms:

Chemical Property of 12-{2-[bis(but-2-ynyl)amino]phenoxy}dodecanenitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 12-{2-[bis(but-2-ynyl)amino]phenoxy}dodecanenitrile

There total 3 articles about 12-{2-[bis(but-2-ynyl)amino]phenoxy}dodecanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-phenol (95-55-6) → 12-{2-[bis(but-2-ynyl)amino]phenoxy}dodecanenitrile (1365564-03-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 0 - 50 °C / Inert atmosphere

2: potassium carbonate / acetone / Inert atmosphere; Reflux

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; acetone;

DOI:10.1016/j.tet.2012.01.046

Reference yield:

12-bromododecanenitrile (54863-47-7) → 12-{2-[bis(but-2-ynyl)amino]phenoxy}dodecanenitrile (1365564-03-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 0 - 50 °C / Inert atmosphere

2: potassium carbonate / acetone / Inert atmosphere; Reflux

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; acetone;

DOI:10.1016/j.tet.2012.01.046

Reference yield:

C18H28N2O + 1-Bromo-2-butyne (3355-28-0) → 12-{2-[bis(but-2-ynyl)amino]phenoxy}dodecanenitrile (1365564-03-9)

Guidance literature:

With potassium carbonate; In acetone; Inert atmosphere; Reflux;

DOI:10.1016/j.tet.2012.01.046

upstream raw materials:

1-Bromo-2-butyne

2-amino-phenol

12-bromododecanenitrile

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