Technology Process of C47H57NO15
There total 5 articles about C47H57NO15 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran; water;
at 0 - 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/jm400479p
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 10 h / -40 °C / Inert atmosphere
2.1: pyridinium chlorochromate / dichloromethane / 8 h / 20 °C / Inert atmosphere
3.1: hydrogen fluoride; pyridine / water; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
4.2: Inert atmosphere
5.1: hydrogenchloride / water; tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
With
pyridine; 1H-imidazole; hydrogenchloride; hydrogen fluoride; sodium hexamethyldisilazane; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm400479p
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen fluoride; pyridine / water; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: hydrogenchloride / water; tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
With
pyridine; hydrogenchloride; hydrogen fluoride; sodium hexamethyldisilazane;
In
tetrahydrofuran; water;
DOI:10.1021/jm400479p
