C₅₀H₉₂N₂O₃Si₃

Base Information

Chemical Name:C₅₀H₉₂N₂O₃Si₃
CAS No.:1439381-99-3
Molecular Formula:C₅₀H₉₂N₂O₃Si₃
Molecular Weight:853.549
Hs Code.:

C<sub>50</sub>H<sub>92</sub>N<sub>2</sub>O<sub>3</sub>Si<sub>3</sub>

Synonyms:

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Chemical Property of C₅₀H₉₂N₂O₃Si₃

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Technology Process of C₅₀H₉₂N₂O₃Si₃

There total 18 articles about C₅₀H₉₂N₂O₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4E)-(1R,3aR,7aR)-1-[(2R)-6-(triethylsilyloxy)-6-methylheptan-2-yl]-4-bromomethylene-7a-methyloctahydro-1H-indene

: 1439381-93-7
(3R,4S,5R)-3,5-bis(tert-butyldimethylsilyloxy)-4-[2-(imidazol-1-yl)ethyl]oct-1-en-7-yne

: 1439381-99-3
C₅₀H₉₂N₂O₃Si₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In toluene; at 110 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ml400098w

Reference yield:

: methyl 4,6-O-benzylidene-3-deoxy-3-C-ethenyl-α-D-altropyranoside

: 1439381-99-3
C₅₀H₉₂N₂O₃Si₃

Guidance literature:: Multi-step reaction with 15 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide; dihydrogen peroxide / 16 h / 20 °C / Inert atmosphere

4.1: pyridine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

5.1: barium carbonate; N-Bromosuccinimide / tetrachloromethane / 2 h / 0 °C / Reflux

6.1: sodium cyanoborohydride; zinc / propan-1-ol; water / 0.67 h / 20 °C / Reflux

7.1: pyridine / 15.5 h / 0 - 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

9.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

9.2: 2 h / -78 - 20 °C / Inert atmosphere

10.1: potassium carbonate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere

11.1: 2,6-dimethylpyridine / dichloromethane / 17 h / 0 - 20 °C / Inert atmosphere

12.1: diisobutylaluminium hydride / dichloromethane; toluene / 2.5 h / -78 °C / Inert atmosphere

12.2: 1 h / -78 - 20 °C

13.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

14.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

14.2: 59 h / 0 °C / Inert atmosphere; Reflux

15.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 1 h / 110 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; potassium carbonate; triethylamine; barium carbonate; sodium hydroxide; zinc; In tetrahydrofuran; methanol; propan-1-ol; tetrachloromethane; hexane; dichloromethane; water; toluene; mineral oil;
DOI:10.1021/ml400098w

Reference yield:

: 1439381-92-6
(3R,4S,5R)-3,5-bis(tert-butyldimethylsilyloxy)-4-[2-(mesyloxy)-ethyl]oct-1-en-7-yne

: 1439381-99-3
C₅₀H₉₂N₂O₃Si₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 59 h / 0 °C / Inert atmosphere; Reflux

2.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 1 h / 110 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; triethylamine; In tetrahydrofuran; toluene; mineral oil;
DOI:10.1021/ml400098w