cholesteryl (3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside)

Base Information

Chemical Name:cholesteryl (3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside)
CAS No.:144101-17-7
Molecular Formula:C₅₄H₇₄O₅
Molecular Weight:803.179
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cholesteryl (3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside)

Chemical Property:

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Technology Process of cholesteryl (3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside)

There total 9 articles about cholesteryl (3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 144101-01-9,144101-08-6,144101-09-7
C₆₁H₈₀O₆S

: 144101-16-6,144101-17-7
(2R,3R,4R,6R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-6-[(3S,8S,9S,10R,13R,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yloxy]-tetrahydro-pyran

Guidance literature:: With W-2 Raney nickel; In tetrahydrofuran; ethanol; at 23 ℃; for 3h;
DOI:10.1246/cl.1992.1511

Reference yield: 68.0%

: 144101-01-9,144101-08-6,144101-09-7
C₆₁H₈₀O₆S

: 144101-16-6,144101-17-7
(2R,3S,4R,6R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-6-[(3S,8S,9S,10R,13R,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yloxy]-tetrahydro-pyran

Guidance literature:: With W-2 Raney nickel; In tetrahydrofuran; ethanol; at 23 ℃; for 3h;
DOI:10.1246/cl.1992.1511

Reference yield:

: 57-88-5
cholesterol

: 80040-79-5
3,4,6-tri-O-benzyl-D-galactal

: 380450-56-6
cholesteryl (2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexapyranosyl)

: 144101-17-7
cholesteryl (3,4,6-tri-O-benzyl-2-deoxy-β-D-galactopyranoside)

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In toluene; at 50 ℃; for 0.0833333h; Overall yield = 82 percent; Overall yield = 158 mg; stereoselective reaction; Inert atmosphere;
DOI:10.1039/d0ob01042a