2-isopropoxyphenolato-magnesium tetrahydroborate diethyl ether (1/2)

Base Information

• Chemical Name: 2-isopropoxyphenolato-magnesium tetrahydroborate diethyl ether (1/2)
• CAS No.: 862776-00-9
• Molecular Formula: C₁₇H₃₅BMgO₄
• Molecular Weight: 338.578
• Mol file: 862776-00-9.mol

Synonyms:

Chemical Property of 2-isopropoxyphenolato-magnesium tetrahydroborate diethyl ether (1/2)

Chemical Property:

Purity/Quality:

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Technology Process of 2-isopropoxyphenolato-magnesium tetrahydroborate diethyl ether (1/2)

There total 1 articles about 2-isopropoxyphenolato-magnesium tetrahydroborate diethyl ether (1/2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.5%

diethyl ether (60-29-7,927820-24-4) + ethyl-magnesium tetrahydroborate (6077-70-9,18129-13-0) + 2-Isopropoxyphenol (4812-20-8) → 2-isopropoxyphenolato-magnesium tetrahydroborate diethyl ether (1/2) (862776-00-9)

Guidance literature:

In diethyl ether; byproducts: C2H6; all manipulations under anhydrous conditions and under N2 atm.; soln. oforg. compd. added dropwise to stirred soln. of Mg compd.; filtered, washed with Et2O, dried in vac.; elem. anal.;

DOI:10.1002/zaac.200400420

upstream raw materials:

diethyl ether

ethyl-magnesium tetrahydroborate

2-Isopropoxyphenol

Refernces