C₁₇H₁₉NO₂S

Base Information

• Chemical Name: C₁₇H₁₉NO₂S
• CAS No.: 1402168-29-9
• Molecular Formula: C₁₇H₁₉NO₂S
• Molecular Weight: 301.409
• Mol file: 1402168-29-9.mol

Synonyms:

Chemical Property of C₁₇H₁₉NO₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₉NO₂S

There total 1 articles about C₁₇H₁₉NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-tert-butylbenzyl)benzenesulfonamide (1022379-81-2) → C17H19NO2S (1402168-29-9)

Guidance literature:

N-(4-tert-butylbenzyl)benzenesulfonamide; With tert-butylhypochlorite; sodium sulfate; potassium bromide; In acetonitrile; at 20 ℃; for 1h;

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In acetonitrile; at 20 ℃; for 0.5h;

With sodium carbonate; In acetonitrile; at 20 ℃; for 20h;

DOI:10.1002/anie.201607223

Reference yield: 22.0%

C17H19NO2S (1402168-29-9) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → C77H21NO2S (1402168-44-8) + 1,2-Dihydro<60>fullerene (142482-13-1,469865-72-3)

Guidance literature:

With dibromobis(triphenylphosphine)nickel(II); water; zinc; In 1,2-dichloro-benzene; at 120 ℃; for 24h; Inert atmosphere; sealed tube;

DOI:10.1002/ejoc.201200055

Reference yield:

trimethylsilyl cyanide (7677-24-9) + C17H19NO2S (1402168-29-9) → N-((4-(tert-butyl)phenyl)(cyano)methyl)benzenesulfonamide

Guidance literature:

With lithium perchlorate; In acetonitrile; at 20 ℃;

DOI:10.1002/anie.201607223

upstream raw materials:

N-(4-tert-butylbenzyl)benzenesulfonamide

Downstream raw materials:

C₇₇H₂₁NO₂S

1,2-Dihydro<60>fullerene