C₂₁H₁₇N₃OS

Base Information

Chemical Name:C₂₁H₁₇N₃OS
CAS No.:1418012-76-6
Molecular Formula:C₂₁H₁₇N₃OS
Molecular Weight:359.451
Hs Code.:

C<sub>21</sub>H<sub>17</sub>N<sub>3</sub>OS

Synonyms:

Suppliers and Price of C₂₁H₁₇N₃OS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₁₇N₃OS

Chemical Property:

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Technology Process of C₂₁H₁₇N₃OS

There total 7 articles about C₂₁H₁₇N₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-59-8
2-phenoxyacetic acid

: 1418012-76-6
C₂₁H₁₇N₃OS

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / 3 h / Reflux

2.1: hydrazine hydrate / ethanol / 3 h / Reflux

3.1: ethanol / 1 h / Reflux

4.1: sodium hydroxide / 1 h / Reflux

5.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

7.1: sodium hydride / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

7.2: 5 h / 20 °C / Inert atmosphere

With sodium hydride; potassium carbonate; toluene-4-sulfonic acid; hydrazine hydrate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm3013213

Reference yield:

: 129544-78-1
3-Methylsulfanyl-5-phenoxymethyl-4-phenyl-4H-[1,2,4]triazole

: 1418012-76-6
C₂₁H₁₇N₃OS

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

2.2: 5 h / 20 °C / Inert atmosphere

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm3013213

Reference yield:

: 21358-13-4
2-[3-phenoxymethyl-4-phenyl-1,2,4-triazole]-5-thiol

: 1418012-76-6
C₂₁H₁₇N₃OS

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

3.1: sodium hydride / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

3.2: 5 h / 20 °C / Inert atmosphere

With sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm3013213