C₂₅H₂₉N₃O₃S

Base Information

Chemical Name:C₂₅H₂₉N₃O₃S
CAS No.:1374355-11-9
Molecular Formula:C₂₅H₂₉N₃O₃S
Molecular Weight:451.59
Hs Code.:

C<sub>25</sub>H<sub>29</sub>N<sub>3</sub>O<sub>3</sub>S

Synonyms:

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Chemical Property of C₂₅H₂₉N₃O₃S

Chemical Property:

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Technology Process of C₂₅H₂₉N₃O₃S

There total 17 articles about C₂₅H₂₉N₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 913829-25-1
2-(methylthio)-6-{[(triisopropylsilyl)oxy]methyl}nicotinonitrile

: 1374355-11-9
C₂₅H₂₉N₃O₃S

Guidance literature:: Multi-step reaction with 14 steps

1: 3-chloro-benzenecarboperoxoic acid / ethanol

2: ethylmagnesium bromide / diethyl ether

3: diisobutylaluminium hydride / toluene

5: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran

6: N-Bromosuccinimide / tetrahydrofuran

7: sodium diformamide / acetonitrile

8: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

9: 1H-imidazole / N,N-dimethyl-formamide

10: Lawessons reagent; pyridine / toluene / 100 °C

11: tetrabutyl ammonium fluoride / tetrahydrofuran

12: thionyl chloride / toluene

13: N-ethyl-N,N-diisopropylamine / acetonitrile

14: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; 1H-imidazole; N-Bromosuccinimide; thionyl chloride; ethylmagnesium bromide; sodium diformamide; tetrabutyl ammonium fluoride; water; sodium hexamethyldisilazane; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; chloroform; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: 185147-08-4
4-fluoro-3-methylbenzonitrile

: 1374355-11-9
C₂₅H₂₉N₃O₃S

Guidance literature:: Multi-step reaction with 9 steps

1: sodium hydride

2: sodium hydroxide

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

4: 1H-imidazole / N,N-dimethyl-formamide

5: Lawessons reagent; pyridine / toluene / 100 °C

6: tetrabutyl ammonium fluoride / tetrahydrofuran

7: thionyl chloride / toluene

8: N-ethyl-N,N-diisopropylamine / acetonitrile

9: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; 1H-imidazole; thionyl chloride; tetrabutyl ammonium fluoride; water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; chloroform; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: 175277-27-7
6-formyl-2-(methylthio)nicotinonitrile

: 1374355-11-9
C₂₅H₂₉N₃O₃S

Guidance literature:: Multi-step reaction with 16 steps

1: sodium tetrahydroborate

2: 1H-imidazole

3: 3-chloro-benzenecarboperoxoic acid / ethanol

4: ethylmagnesium bromide / diethyl ether

5: diisobutylaluminium hydride / toluene

7: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran

8: N-Bromosuccinimide / tetrahydrofuran

9: sodium diformamide / acetonitrile

10: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

11: 1H-imidazole / N,N-dimethyl-formamide

12: Lawessons reagent; pyridine / toluene / 100 °C

13: tetrabutyl ammonium fluoride / tetrahydrofuran

14: thionyl chloride / toluene

15: N-ethyl-N,N-diisopropylamine / acetonitrile

16: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; 1H-imidazole; sodium tetrahydroborate; N-Bromosuccinimide; thionyl chloride; ethylmagnesium bromide; sodium diformamide; tetrabutyl ammonium fluoride; water; sodium hexamethyldisilazane; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; chloroform; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067