potassium 2-(morpholine-4-carbonyl)phenyltrifluoroborate

Base Information

Chemical Name:potassium 2-(morpholine-4-carbonyl)phenyltrifluoroborate
CAS No.:1386231-41-9
Molecular Formula:C₁₁H₁₂BF₃NO₂*K
Molecular Weight:297.126
Hs Code.:

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Chemical Property of potassium 2-(morpholine-4-carbonyl)phenyltrifluoroborate

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Technology Process of potassium 2-(morpholine-4-carbonyl)phenyltrifluoroborate

There total 3 articles about potassium 2-(morpholine-4-carbonyl)phenyltrifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 6392-26-3
(2-chlorophenyl)(morpholino)methanone

: 1279123-63-5
potassium hydrogenfluoride

: 13675-18-8
tetrahydroxydiboron

: 1386231-41-9
potassium 2-(morpholine-4-carbonyl)phenyltrifluoroborate

Guidance literature:: With PdCl(C₆H₄C₆H₄NH₂)(Cy₂PC₆H₄-2-C₆H₂-2',4',6'-i-Pr₃); Cy₂PC₆H₄-2-C₆H₂-2',4',6'-i-Pr₃; K acetate; In ethanol; aryl chloride reacted with B2(OH)4 in EtOH in presence of catalyst (Pt-complex - ligand) and K acetate at 80°C for 4 h; subjected to aq. workup; treated with KHF2; purified by Soxlet extn.;
DOI:10.1021/ja303181m

Reference yield:

: 874219-17-7
[2-(morpholin-4-ylcarbonyl)phenyl]boronic acid

: 1386231-41-9
potassium 2-(morpholine-4-carbonyl)phenyltrifluoroborate

Guidance literature:: With potassium hydrogenfluoride; In methanol; water; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja303181m

Reference yield:

: 6392-26-3
(2-chlorophenyl)(morpholino)methanone

: 1386231-41-9
potassium 2-(morpholine-4-carbonyl)phenyltrifluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydroxydiboron; (chloro(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II)); potassium acetate; XPhos / ethanol / 4 h / 80 °C / Inert atmosphere

2: potassium hydrogenfluoride / methanol; water / 0.5 h / 0 - 20 °C / Inert atmosphere

With potassium hydrogenfluoride; tetrahydroxydiboron; (chloro(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II)); potassium acetate; XPhos; In methanol; ethanol; water;
DOI:10.1021/ja303181m