V(SC₆H₃-2,6-(SiMe₃)2)3(THF)

Base Information

• Chemical Name: V(SC₆H₃-2,6-(SiMe₃)2)3(THF)
• CAS No.: 843663-56-9
• Molecular Formula: C₄₀H₇₁OS₃Si₆V
• Molecular Weight: 883.656

Synonyms:

Chemical Property of V(SC₆H₃-2,6-(SiMe₃)2)3(THF)

Chemical Property:

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Technology Process of V(SC₆H₃-2,6-(SiMe₃)2)3(THF)

There total 1 articles about V(SC₆H₃-2,6-(SiMe₃)2)3(THF) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Vanadium (III) chloride-(tris-tetrahydrofuran) (131063-11-1,16997-51-6,19559-06-9) + lithium 2,6-bis(trimethylsilyl)phenylthiolate → V(SC6H3-2,6-(SiMe3)2)3 + V(SC6H3-2,6-(SiMe3)2)3(THF) (843663-56-9)

Guidance literature:

In toluene; addn. of 3 equivs. of lithium salt to vanadium complex in toluene at 60°C; evapn., extn. with hexamethyldisiloxane, crystn.;

DOI:10.1021/ic048721c

Reference yield: 76.0%

N,N,N,N,-tetramethylethylenediamine (110-18-9) + V(SC6H3-2,6-(SiMe3)2)3(THF) (843663-56-9) → [V(SC6H3(Si(CH3)3)2)CH2Si(CH3)2C6H3S(Si(CH3)3)((CH3)2NCH2CH2N(CH3)2)]

Guidance literature:

In not given;

DOI:10.1021/ic048721c

Reference yield: 73.0%

V(SC6H3-2,6-(SiMe3)2)3(THF) (843663-56-9) + 1-Azidoadamantane (24886-73-5) → V(SC6H3-2,6-(SiMe3)2)3(NC10H15)

Guidance literature:

In toluene; byproducts: N2; addn. of azide to soln. of vanadium complex in toluene at room temp.;

DOI:10.1021/ic048721c

upstream raw materials:

Vanadium (III) chloride-(tris-tetrahydrofuran)

Downstream raw materials:

[V(SC₆H₃(Si(CH₃)3)2)NC₆H₅(CH₂Si(CH₃)2C₆H₃SNC₆H₅(Si(CH₃)3))]

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