C₄₃H₆₀N₂O₈

Base Information

Chemical Name:C₄₃H₆₀N₂O₈
CAS No.:1446749-29-6
Molecular Formula:C₄₃H₆₀N₂O₈
Molecular Weight:732.958
Hs Code.:

C<sub>43</sub>H<sub>60</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₄₃H₆₀N₂O₈

Chemical Property:

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Technology Process of C₄₃H₆₀N₂O₈

There total 11 articles about C₄₃H₆₀N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1446749-05-8
C₂₇H₄₅N₃O₁₁Si

: 1446749-29-6
C₄₃H₆₀N₂O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium methylate / dichloromethane; methanol / 0.5 h / 20 °C

1.2: IR-120 resin

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

2.2: 2 h / 0 - 20 °C

3.1: triphenylphosphine / tetrahydrofuran; water / 12 h / 20 °C

4.1: pyridine / 12 h / 0 - 20 °C

5.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

6.1: lead(IV) tetraacetate; sodium carbonate / dichloromethane / 1 h / 0 - 20 °C

7.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 3.5 h / 0 - 20 °C

8.1: pyridine

9.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C

10.1: sodium methylate / methanol

10.2: IR-120 resin

With pyridine; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; sodium methylate; lead(IV) tetraacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201204550

Reference yield:

: 100-39-0
benzyl bromide

: 1446749-29-6
C₄₃H₆₀N₂O₈

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

1.2: 2 h / 0 - 20 °C

2.1: triphenylphosphine / tetrahydrofuran; water / 12 h / 20 °C

3.1: pyridine / 12 h / 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

5.1: lead(IV) tetraacetate; sodium carbonate / dichloromethane / 1 h / 0 - 20 °C

6.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 3.5 h / 0 - 20 °C

7.1: pyridine

8.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C

9.1: sodium methylate / methanol

9.2: IR-120 resin

With pyridine; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; sodium methylate; lead(IV) tetraacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201204550

Reference yield:

: 1446749-26-3
C₄₄H₆₁NO₉Si

: 1446749-29-6
C₄₃H₆₀N₂O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

2.1: lead(IV) tetraacetate; sodium carbonate / dichloromethane / 1 h / 0 - 20 °C

3.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 3.5 h / 0 - 20 °C

4.1: pyridine

5.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C

6.1: sodium methylate / methanol

6.2: IR-120 resin

With pyridine; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; sodium methylate; lead(IV) tetraacetate; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/chem.201204550