Technology Process of C18H14N2O3
There total 3 articles about C18H14N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H16N2O3;
With
lithium hydroxide;
In
tetrahydrofuran; water;
at 20 ℃;
With
hydrogenchloride;
In
tetrahydrofuran; water;
DOI:10.1039/c2ob27114a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
1.2: 4.5 h / 50 °C / Inert atmosphere
2.1: lithium hydroxide / water; tetrahydrofuran / 20 °C
With
N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; lithium hydroxide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob27114a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
1.2: 4.5 h / 50 °C / Inert atmosphere
2.1: lithium hydroxide / water; tetrahydrofuran / 20 °C
With
N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; lithium hydroxide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob27114a
