[Pt2(κ2-C6H4PPh2)2(μ-2-C6H4PPh2)2] C72H56P4Pt2, orthorhombic

Base Information

Chemical Name:[Pt2(κ2-C6H4PPh2)2(μ-2-C6H4PPh2)2] C72H56P4Pt2, orthorhombic
CAS No.:63672-46-8
Molecular Formula:C₇₂H₅₆P₄Pt₂
Molecular Weight:1435.29
Hs Code.:

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Chemical Property of [Pt2(κ2-C6H4PPh2)2(μ-2-C6H4PPh2)2] C72H56P4Pt2, orthorhombic

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Technology Process of [Pt2(κ2-C6H4PPh2)2(μ-2-C6H4PPh2)2] C72H56P4Pt2, orthorhombic

There total 4 articles about [Pt2(κ2-C6H4PPh2)2(μ-2-C6H4PPh2)2] C72H56P4Pt2, orthorhombic which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: cis-[Pt(κ²-2-C₆H₄PPh₂)₂]

: 63672-46-8,949459-37-4
[Pt2(κ2-C6H4PPh2)2(μ-2-C6H4PPh2)2] C72H56P4Pt2, orthorhombic

Guidance literature:: In toluene; under inert atm. soln. Pt complex in toluene was stirred for 24 h at bath temp. 130 °C for 24 h; mixt. was concd. in vac., chromy. on silica; elem. anal.;
DOI:10.1039/b702808c

Reference yield: 40.0%

: 949155-23-1
[Pt(κ(2)P,C-C6H3-5-Me-2-PPh2)2]

: [Pt2(κ2-2-C6H4PPh2)(μ-2-C6H4PPh2)2]n

: 63672-46-8,949459-37-4
[Pt2(κ2-C6H4PPh2)2(μ-2-C6H4PPh2)2] C72H56P4Pt2, orthorhombic

Guidance literature:: With CO; In benzene; under CO atm. soln. Pt complex in benzene was stirred for 48 h at room temp.;
DOI:10.1039/b702808c

Reference yield:

: 321658-65-5
(2-Br-4-MeC₆H₃)PPh₂

: 63672-46-8,949459-37-4
[Pt2(κ2-C6H4PPh2)2(μ-2-C6H4PPh2)2] C72H56P4Pt2, orthorhombic

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi / hexane

2: CO / benzene

With n-BuLi; CO; In hexane; benzene;
DOI:10.1039/b702808c