Technology Process of C34H29N3O5S2
There total 2 articles about C34H29N3O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
Darkness;
DOI:10.1021/ml300191g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C
2: tetrabutyl-ammonium chloride; lithium chloride; lithium acetate; palladium diacetate / N,N-dimethyl-formamide / 100 °C
3: hydrogenchloride; water / tetrahydrofuran / 3 h / 60 °C
4: sodium cyanide / methanol / 20 °C / Darkness
5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere; Darkness
With
hydrogenchloride; dmap; sodium cyanide; lithium acetate; tetrabutyl-ammonium chloride; water; palladium diacetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; lithium chloride; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
1: |Mitsunobu Displacement / 2: |Heck Reaction;
DOI:10.1021/ml300191g