p-xylylenebis(triphenylphosphonium)hexachlorozirconate

Base Information

• Chemical Name: p-xylylenebis(triphenylphosphonium)hexachlorozirconate
• CAS No.: 143568-31-4
• Molecular Formula: C₄₄H₃₈P₂*Cl₆Zr
• Molecular Weight: 932.675
• Mol file: 143568-31-4.mol

Synonyms:

Chemical Property of p-xylylenebis(triphenylphosphonium)hexachlorozirconate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of p-xylylenebis(triphenylphosphonium)hexachlorozirconate

There total 1 articles about p-xylylenebis(triphenylphosphonium)hexachlorozirconate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-xylenebis(triphenylphosphonium) dibromide (40817-03-6) + zirconium(IV) chloride (10026-11-6) → p-xylylenebis(triphenylphosphonium)hexachlorozirconate (143568-31-4)

Guidance literature:

With hydrogenchloride; In ethanol; ZrCl4 is dissolved in EtOH and HCl gas passed into the soln. until a pick-up of 15 % w/w is obtained, addn. a suspn. of bis(triphenylphosphonium bromide)paraxylene in EtOH to the cooled soln., stirring for 24 h (nitrogen atmosphere, Schlenk tube); the crystalline material is separated by filtn., washed with ether and dried in vac., elem. anal.;

DOI:10.1016/0925-8388(92)90554-M

upstream raw materials:

p-xylenebis(triphenylphosphonium) dibromide

zirconium(IV) chloride