C₄₀H₄₇O₁₂P

Base Information

Chemical Name:C₄₀H₄₇O₁₂P
CAS No.:1403669-32-8
Molecular Formula:C₄₀H₄₇O₁₂P
Molecular Weight:750.78
Hs Code.:

C<sub>40</sub>H<sub>47</sub>O<sub>12</sub>P

Synonyms:

Suppliers and Price of C₄₀H₄₇O₁₂P

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₀H₄₇O₁₂P

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₀H₄₇O₁₂P

There total 6 articles about C₄₀H₄₇O₁₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158414-26-7
(2R,3R,4S,5S,6R)-4,5-bis(benzyloxy)-6-((benzyloxy)methyl)-3-hydroxy-2-methoxy-1,2-oxaphosphinane-2-oxide

: 1403669-32-8
C₄₀H₄₇O₁₂P

Guidance literature:: Multi-step reaction with 7 steps

1: n-Bu₄NHSO₄; sodium hydroxide / dichloromethane / 1.5 h / Inert atmosphere; Reflux

2: Lawessons reagent / toluene / 24 h / 70 °C / Inert atmosphere

3: dimethylsulfide borane complex / tetrahydrofuran / 3.5 h / Inert atmosphere

4: thiophenol / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

5: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; 4-nitro-1H-1,2,3-triazole / tetrahydrofuran; toluene / 20 °C / Inert atmosphere

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

7: methanol; sodium methylate / 20 h / 20 °C / Inert atmosphere

With Lawessons reagent; methanol; dimethylsulfide borane complex; n-Bu₄NHSO₄; sodium methylate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; thiophenol; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; 4-nitro-1H-1,2,3-triazole; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja305104b

Reference yield:

: 100-39-0
benzyl bromide

: 1403669-32-8
C₄₀H₄₇O₁₂P

Guidance literature:: Multi-step reaction with 7 steps

1: n-Bu₄NHSO₄; sodium hydroxide / dichloromethane / 1.5 h / Inert atmosphere; Reflux

2: Lawessons reagent / toluene / 24 h / 70 °C / Inert atmosphere

3: dimethylsulfide borane complex / tetrahydrofuran / 3.5 h / Inert atmosphere

4: thiophenol / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

5: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; 4-nitro-1H-1,2,3-triazole / tetrahydrofuran; toluene / 20 °C / Inert atmosphere

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

7: methanol; sodium methylate / 20 h / 20 °C / Inert atmosphere

With Lawessons reagent; methanol; dimethylsulfide borane complex; n-Bu₄NHSO₄; sodium methylate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; thiophenol; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; 4-nitro-1H-1,2,3-triazole; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja305104b

Reference yield:

: 1384982-02-8
(2R,3R,4S,5S,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)-2-methoxy-1,2-oxaphosphinane-2-oxide

: 1403669-32-8
C₄₀H₄₇O₁₂P

Guidance literature:: Multi-step reaction with 6 steps

1: Lawessons reagent / toluene / 24 h / 70 °C / Inert atmosphere

2: dimethylsulfide borane complex / tetrahydrofuran / 3.5 h / Inert atmosphere

3: thiophenol / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

4: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; 4-nitro-1H-1,2,3-triazole / tetrahydrofuran; toluene / 20 °C / Inert atmosphere

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

6: methanol; sodium methylate / 20 h / 20 °C / Inert atmosphere

With Lawessons reagent; methanol; dimethylsulfide borane complex; sodium methylate; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; thiophenol; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 4-nitro-1H-1,2,3-triazole; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja305104b