3-oxo-6,7-seco-5β-cholane-6,7,24-trioic acid

Base Information

Chemical Name:3-oxo-6,7-seco-5β-cholane-6,7,24-trioic acid
CAS No.:95749-50-1
Molecular Formula:C₂₄H₃₆O₇
Molecular Weight:436.546
Hs Code.:

Synonyms:

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Chemical Property of 3-oxo-6,7-seco-5β-cholane-6,7,24-trioic acid

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Technology Process of 3-oxo-6,7-seco-5β-cholane-6,7,24-trioic acid

There total 8 articles about 3-oxo-6,7-seco-5β-cholane-6,7,24-trioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4651-67-6
7-Ketolithocholic acid

: 95749-50-1,123166-29-0
3-oxo-6,7-seco-5β-cholane-6,7,24-trioic acid

Guidance literature:: Multi-step reaction with 6 steps

1: HCl

2: pyridine

3: bromine; HBr; acetic acid

4: aqueous methanol. KOH / 20 °C

5: aluminium isopropylate; isopropyl alcohol

6: CrO₃; acetic acid

With pyridine; chromium(VI) oxide; hydrogenchloride; potassium hydroxide; hydrogen bromide; bromine; aluminum isopropoxide; acetic acid; isopropyl alcohol;

Reference yield:

: 10538-59-7
7-ketolithocholic methyl ester

: 95749-50-1,123166-29-0
3-oxo-6,7-seco-5β-cholane-6,7,24-trioic acid

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine

2: bromine; HBr; acetic acid

3: aqueous methanol. KOH / 20 °C

4: aluminium isopropylate; isopropyl alcohol

5: CrO₃; acetic acid

With pyridine; chromium(VI) oxide; potassium hydroxide; hydrogen bromide; bromine; aluminum isopropoxide; acetic acid; isopropyl alcohol;

Reference yield:

: 10452-65-0
methyl 3α-acetoxy-7-oxo-5β-cholan-24-oate

: 95749-50-1,123166-29-0
3-oxo-6,7-seco-5β-cholane-6,7,24-trioic acid

Guidance literature:: Multi-step reaction with 4 steps

1: bromine; HBr; acetic acid

2: aqueous methanol. KOH / 20 °C

3: aluminium isopropylate; isopropyl alcohol

4: CrO₃; acetic acid

With chromium(VI) oxide; potassium hydroxide; hydrogen bromide; bromine; aluminum isopropoxide; acetic acid; isopropyl alcohol;