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Gold, chloro(dicyclohexylphosphine)-

Base Information
  • Chemical Name:Gold, chloro(dicyclohexylphosphine)-
  • CAS No.:127690-39-5
  • Molecular Formula:C12H23AuClP
  • Molecular Weight:430.708
  • Hs Code.:
Gold, chloro(dicyclohexylphosphine)-

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Chemical Property of Gold, chloro(dicyclohexylphosphine)-
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Technology Process of Gold, chloro(dicyclohexylphosphine)-

There total 1 articles about Gold, chloro(dicyclohexylphosphine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In diethyl ether; byproducts: CO; in carbon monoxide atmosphere; reaction temp.: 25°C; 10-50% excess of ligand is successful; reaction mixt. was evapd.; product was filtered; washed and dried; elem. anal.; IR; NMR;
Guidance literature:
With aq. NH4OH; In tetrahydrofuran; aq. NH4OH added to a soln. of Au-comp. in THF, stirred for 30 min; solv. removed, washed with H2O, recrystd. from toluene;
DOI:10.1002/anie.200390270
Guidance literature:
With aq. ammonia; In tetrahydrofuran; water; under N2; aq. ammonia added to soln. of Au complex in THF; stirred for 15 min; filtered; mixt. of (Au(PCy2))(n) compds. obtained; recrystd. from toluene-MeCN or heated in toluene (mixt. of two compds.); evapd. slowly from toluene; occasionally (Au(PCy2))6*C7H8 isolated; elem. anal.;
DOI:10.1021/ic035006e
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