C₂₃H₁₆OS

Base Information

Chemical Name:C₂₃H₁₆OS
CAS No.:1527009-85-3
Molecular Formula:C₂₃H₁₆OS
Molecular Weight:340.445
Hs Code.:

Synonyms:

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Chemical Property of C₂₃H₁₆OS

Chemical Property:

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Technology Process of C₂₃H₁₆OS

There total 7 articles about C₂₃H₁₆OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₀O₃S₂

: 1527009-85-3
C₂₃H₁₆OS

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene / 24 h / 120 °C / Inert atmosphere; Schlenk technique

2: acetic acid; dihydrogen peroxide / Inert atmosphere; Schlenk technique

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; sodium carbonate; acetic acid; In water; toluene; 1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol402971n

Reference yield:

: 1714-29-0
1-bromopyrene

: 1527009-85-3
C₂₃H₁₆OS

Guidance literature:: Multi-step reaction with 6 steps

1.1: Inert atmosphere; Schlenk technique

2.1: n-butyllithium / Inert atmosphere; Schlenk technique

2.2: Inert atmosphere; Schlenk technique

3.1: boron tribromide / dichloromethane / Inert atmosphere; Schlenk technique

4.1: triethylamine / Inert atmosphere; Schlenk technique

5.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene / 24 h / 120 °C / Inert atmosphere; Schlenk technique

6.1: acetic acid; dihydrogen peroxide / Inert atmosphere; Schlenk technique

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; dihydrogen peroxide; boron tribromide; sodium carbonate; acetic acid; triethylamine; In dichloromethane; water; toluene; 5.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol402971n

Reference yield:

: 34246-96-3
1-methoxypyrene

: 1527009-85-3
C₂₃H₁₆OS

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / Inert atmosphere; Schlenk technique

1.2: Inert atmosphere; Schlenk technique

2.1: boron tribromide / dichloromethane / Inert atmosphere; Schlenk technique

3.1: triethylamine / Inert atmosphere; Schlenk technique

4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; toluene / 24 h / 120 °C / Inert atmosphere; Schlenk technique

5.1: acetic acid; dihydrogen peroxide / Inert atmosphere; Schlenk technique

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; dihydrogen peroxide; boron tribromide; sodium carbonate; acetic acid; triethylamine; In dichloromethane; water; toluene; 4.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol402971n