Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate

Base Information

Chemical Name:Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate
CAS No.:118246-93-8
Molecular Formula:C₂₀H₂₄NO₄S₂*Na
Molecular Weight:429.537
Hs Code.:

Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate

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Technology Process of Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate

There total 3 articles about Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 118226-54-3
5-(1,2-O-isopropylidene-α-D-xylo-tetrafuranos-4-yl)-3-(2,4,6-trimethylphenyl)-2-isoxazoline

: 118246-93-8
Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate

Guidance literature:: With 1H-imidazole; sodium hydride; methyl iodide; In tetrahydrofuran; at 10 ℃;
DOI:10.1021/jo00265a016

Reference yield:

: 7284-07-3
5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-eno-furanose

: 118246-93-8
Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / Ambient temperature

2: NaH, methyl iodide, imidazole / tetrahydrofuran / 10 °C

With 1H-imidazole; sodium hydride; methyl iodide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00265a016

Reference yield:

: 2904-57-6
mesitylenecarbonitrile oxide

: 118246-93-8
Sodium; (3aR,5S,6S,6aR)-2,2-dimethyl-5-[(R)-3-(2,4,6-trimethyl-phenyl)-4,5-dihydro-isoxazol-5-yl]-tetrahydro-furo[2,3-d][1,3]dioxole-6-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / Ambient temperature

2: NaH, methyl iodide, imidazole / tetrahydrofuran / 10 °C

With 1H-imidazole; sodium hydride; methyl iodide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00265a016