Hexamethylen-bis-

Base Information

• Chemical Name: Hexamethylen-bis-
• CAS No.: 98170-71-9
• Molecular Formula: C₂₀H₂₈P₂
• Molecular Weight: 330.39
• Mol file: 98170-71-9.mol

Synonyms:

Chemical Property of Hexamethylen-bis-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Hexamethylen-bis-

There total 2 articles about Hexamethylen-bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,6-bis(diphenylphosphino)hexane (19845-69-3) + methyl iodide (74-88-4) → Hexamethylen-bis- (98170-71-9)

Guidance literature:

With tertiary butyl chloride; lithium; Yield given. Multistep reaction; 1.) THF, 0 deg C, ultrasound irradiation, 10 min, 2.) THF, 60 min;

DOI:10.1021/jo00222a025

Reference yield:

1,6-bis(phenylphosphino)hexane (73191-51-2) + methyl iodide (74-88-4) → Hexamethylen-bis- (98170-71-9)

Guidance literature:

Reference yield:

Hexamethylen-bis- (98170-71-9) → Hexamethylen-bis-(methyl-phenyl-phosphin-sulfid) (29023-52-7)

Guidance literature:

With sulfur; In benzene;

upstream raw materials:

1,6-bis(phenylphosphino)hexane

methyl iodide

1,6-bis(diphenylphosphino)hexane

Downstream raw materials:

Hexamethylen-bis-(methyl-phenyl-phosphin-sulfid)