Technology Process of Carbonic acid, (5-nitro-1H-indazol-1-yl)methyl 4-nitrophenyl ester
There total 1 articles about Carbonic acid, (5-nitro-1H-indazol-1-yl)methyl 4-nitrophenyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / water; ethanol / 20 - 85 °C
2: triethylamine / dichloromethane / 1 h / 0 - 20 °C
With
triethylamine; sodium hydroxide;
In
ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.03.075
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dichloromethane
2: 1H-tetrazole / dichloromethane / 20 °C
3: dihydrogen peroxide / dichloromethane; water / 1 h / 0 - 20 °C
4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h / 760.05 Torr / Inert atmosphere
5: dichloromethane / 1 h / 20 °C
6: triphenylphosphine / 1,4-dioxane / 0.5 h / 90 °C
With
1H-tetrazole; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; triphenylphosphine;
In
1,4-dioxane; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.bmcl.2013.03.075
