Acetate₉-methoxy-5,11-dimethyl-2-(4-{3-[4-((5Z,10Z,14Z,19Z)-10,15,20-tri-p-tolyl-porphyrin-5-yl)-phenoxy]-propylcarbamoyl}-butyl)-6H-pyrido[4,3-b]carbazol-2-ium;

Base Information

• Chemical Name: Acetate₉-methoxy-5,11-dimethyl-2-(4-{3-[4-((5Z,10Z,14Z,19Z)-10,15,20-tri-p-tolyl-porphyrin-5-yl)-phenoxy]-propylcarbamoyl}-butyl)-6H-pyrido[4,3-b]carbazol-2-ium
• CAS No.: 124040-08-0
• Molecular Formula: C₂H₃O₂*C₇₃H₆₆N₇O₃
• Molecular Weight: 1148.42

Synonyms:

Chemical Property of Acetate₉-methoxy-5,11-dimethyl-2-(4-{3-[4-((5Z,10Z,14Z,19Z)-10,15,20-tri-p-tolyl-porphyrin-5-yl)-phenoxy]-propylcarbamoyl}-butyl)-6H-pyrido[4,3-b]carbazol-2-ium;

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Acetate₉-methoxy-5,11-dimethyl-2-(4-{3-[4-((5Z,10Z,14Z,19Z)-10,15,20-tri-p-tolyl-porphyrin-5-yl)-phenoxy]-propylcarbamoyl}-butyl)-6H-pyrido[4,3-b]carbazol-2-ium;

There total 7 articles about Acetate₉-methoxy-5,11-dimethyl-2-(4-{3-[4-((5Z,10Z,14Z,19Z)-10,15,20-tri-p-tolyl-porphyrin-5-yl)-phenoxy]-propylcarbamoyl}-butyl)-6H-pyrido[4,3-b]carbazol-2-ium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

<5-<4-(3-aminopropyloxy)phenyl>-10,15,20-tris(4-tolyl)>porphyrin (124040-07-9) + Acetate2-(5-ethoxycarbonyloxy-5-oxo-pentyl)-9-methoxy-5,11-dimethyl-6H-pyrido[4,3-b]carbazol-2-ium; → Acetate9-methoxy-5,11-dimethyl-2-(4-{3-[4-((5Z,10Z,14Z,19Z)-10,15,20-tri-p-tolyl-porphyrin-5-yl)-phenoxy]-propylcarbamoyl}-butyl)-6H-pyrido[4,3-b]carbazol-2-ium; (124040-08-0)

Guidance literature:

With triethylamine; In dichloromethane; for 2h; Heating;

DOI:10.1016/S0040-4020(01)80094-6

Reference yield:

5-(4-hydroxyphenyl)-10,15,20-tris(4-methylphenyl)porphyrin (57412-08-5) → Acetate9-methoxy-5,11-dimethyl-2-(4-{3-[4-((5Z,10Z,14Z,19Z)-10,15,20-tri-p-tolyl-porphyrin-5-yl)-phenoxy]-propylcarbamoyl}-butyl)-6H-pyrido[4,3-b]carbazol-2-ium; (124040-08-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaOH / 1.) DMF, 20 min, RT; 2.) DMF, 4 h RT

2: 47 percent / triethylamine / CH₂Cl₂ / 2 h / Heating

With sodium hydroxide; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(01)80094-6

Reference yield:

ethyl 5-bromovalerate (14660-52-7) → Acetate9-methoxy-5,11-dimethyl-2-(4-{3-[4-((5Z,10Z,14Z,19Z)-10,15,20-tri-p-tolyl-porphyrin-5-yl)-phenoxy]-propylcarbamoyl}-butyl)-6H-pyrido[4,3-b]carbazol-2-ium; (124040-08-0)

Guidance literature:

Multi-step reaction with 5 steps

1: 87 percent / dimethylformamide / 4 h / 120 °C

2: 99 percent / 1M HCl / 3 h / Heating

3: Amberlite IRN-78 in acetate form / methanol / 3 h / Ambient temperature

4: triethylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

5: 47 percent / triethylamine / CH₂Cl₂ / 2 h / Heating

With hydrogenchloride; Amberlite IRN-78 in acetate form; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)80094-6

upstream raw materials:

<5-<4-(3-aminopropyloxy)phenyl>-10,15,20-tris(4-tolyl)>porphyrin

5-(4-hydroxyphenyl)-10,15,20-tris(4-methylphenyl)porphyrin

ethyl 5-bromovalerate

9-methoxyellipticine

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