(3,4,5-Cl₃C₆H₂)3SnBr * Me₂NCOH

Base Information

• Chemical Name: (3,4,5-Cl₃C₆H₂)3SnBr * Me₂NCOH
• CAS No.: 82245-52-1
• Molecular Formula: C₃H₇NO*C₁₈H₆BrCl₉Sn
• Molecular Weight: 813.031
• Mol file: 82245-52-1.mol

Synonyms:

Chemical Property of (3,4,5-Cl₃C₆H₂)3SnBr * Me₂NCOH

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (3,4,5-Cl₃C₆H₂)3SnBr * Me₂NCOH

There total 1 articles about (3,4,5-Cl₃C₆H₂)3SnBr * Me₂NCOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

tetrakis-(3,4,5-trichlorophenyl)stannane (82240-01-5) → (3,4,5-Cl3C6H2)3SnBr * Me2NCOH (82245-52-1)

Guidance literature:

With bromine; N,N-dimethyl-formamide; In N,N-dimethyl-formamide; addn. og soln. of Br2 in DMF to boiling soln. of Sn-compound, cooling; removal of solvent (vac.), treatment with petroleum, filtration off; elem. anal.;

DOI:10.1007/BF00949810

Reference yield: 83.0%

4-Fluorothiophenol (371-42-6) + (3,4,5-Cl3C6H2)3SnBr * Me2NCOH (82245-52-1) → (4-FC6H4S)Sn(3,4,5-Cl3C6H2)3 (78795-74-1)

Guidance literature:

In pyridine; benzene; addn. of C5H5N and 4-FC6H4SH in C6H6 to soln of Sn-compound in C6H6, heating to boiling, cooling; washing (water), drying (CaCl2), removal of solvent (vac.); elem. anal.;

DOI:10.1007/BF00949810

upstream raw materials:

tetrakis-(3,4,5-trichlorophenyl)stannane

Downstream raw materials:

(4-FC₆H₄S)Sn(3,4,5-Cl₃C₆H₂)3