(py)₃MoCl₃

Base Information

• Chemical Name: (py)₃MoCl₃
• CAS No.: 39210-28-1
• Molecular Formula: C₁₅H₁₅Cl₃MoN₃
• Molecular Weight: 439.603
• Mol file: 39210-28-1.mol

Synonyms:

Chemical Property of (py)₃MoCl₃

Chemical Property:

Purity/Quality:

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Technology Process of (py)₃MoCl₃

There total 11 articles about (py)₃MoCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

aluminum hexachloromolybdate → (py)3MoCl3 (13927-99-6,39210-28-1)

Guidance literature:

With pyridine; In ethanol; water; pyridine soln. (ethanol) addn. to aq. Mo-complex soln. (molar ratio Mo:pyridine 1:3), mixt. heating (sand bath) until true soln. formed, pptn. on leaving (vac. desiccator); ppt. washing (ether, acetone, hot ethanol), drying to const. weight (desiccator, over concd. H2SO4); elem. anal.;

Reference yield: 75.0%

3Cs(1+)*Mo2Cl9(3-) = Cs3[Mo2Cl9] → (py)3MoCl3 (13927-99-6,39210-28-1)

Guidance literature:

With pyridine; In pyridine; Electrolysis; heating (200°C, 18 h); pptn. on cooling and treatment with petroleum ether, collection, washing(water, ether), drying (vac.), recrystn. (hot pyridine); elem. anal.;

Reference yield: 75.0%

3Cs(1+)*{Mo2Cl8H}(3-) = Cs3{Mo2Cl8H} → (py)3MoCl3 (13927-99-6,39210-28-1)

Guidance literature:

With pyridine; In pyridine; Electrolysis; heating (200°C, 18 h); pptn. on cooling and treatment with petroleum ether, collection, washing(water, ether), drying (vac.); elem. anal.;

upstream raw materials:

trans-{pyH}{MoCl₄py2}

pyridine

pentachloropyridinemolybdate(III)^(2-)

molybdenum(III) chloride

Downstream raw materials:

Mo(C₅H₅N)(P(C₆H₅)3)2Cl₃