tetramethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

Base Information

• Chemical Name: tetramethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat
• CAS No.: 10210-67-0
• Molecular Formula: C₄H₁₂N*C₂₃H₁₅O₅PV
• Molecular Weight: 527.43
• Mol file: 10210-67-0.mol

Synonyms:

Chemical Property of tetramethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tetramethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

There total 1 articles about tetramethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetracarbonyl bis-(triphenyl phosphine) vanadium (10210-62-5) + tertamethylammonium iodide (75-58-1) → tetramethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat (10210-67-0)

Guidance literature:

With sodium amalgam; In ethanol; shaking a suspension of 3 g (4.36 mmol) V(CO)4(C18H15P)2 in 80 ml ethanol with an excess of Na amalgam (1 % Na) (15-30 minutes) and addition of an excess of a solution of the iodide in water;; precipitation; washing with H2O, ethanol and ether, recrystallization from acetone/ether;;

upstream raw materials:

tetracarbonyl bis-(triphenyl phosphine) vanadium

tertamethylammonium iodide