(1,10-phenanthroline)(triphenylphosphine)dicyanoacetate copper(I)

Base Information

Chemical Name:(1,10-phenanthroline)(triphenylphosphine)dicyanoacetate copper(I)
CAS No.:121151-16-4
Molecular Formula:C₁₂H₈N₂*C₂₂H₁₆CuN₂O₂P
Molecular Weight:615.11
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1,10-phenanthroline)(triphenylphosphine)dicyanoacetate copper(I)

Chemical Property:

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Technology Process of (1,10-phenanthroline)(triphenylphosphine)dicyanoacetate copper(I)

There total 2 articles about (1,10-phenanthroline)(triphenylphosphine)dicyanoacetate copper(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1,10-phenanthroline)(triphenylphosphine)(CH(CN)2)copper(I)

: 124-38-9,18923-20-1
carbon dioxide

: 121151-16-4
(1,10-phenanthroline)(triphenylphosphine)dicyanoacetate copper(I)

Guidance literature:: With P(C₆H₅)3; In dichloromethane; react. time 0.5h; ppt. filtered off under CO2; dried at atm. pressure; elem. anal.;
DOI:10.1016/0022-328X(88)80403-0

Reference yield:

: 114502-36-2
(1,10-phenanthroline)(triphenylphosphine)bicarbonato copper (I)

: 124-38-9,18923-20-1
carbon dioxide

: 109-77-3
malononitrile

: 121151-16-4
(1,10-phenanthroline)(triphenylphosphine)dicyanoacetate copper(I)

Guidance literature:: With P(C₆H₅)3; In toluene; react. time 2h; ppt. filtered off; washed with toluene and Et2O; dried under CO2; elem. anal.;
DOI:10.1016/0022-328X(88)80403-0

Reference yield:

: 121151-16-4
(1,10-phenanthroline)(triphenylphosphine)dicyanoacetate copper(I)

: (1,10-phenanthroline)(triphenylphosphine)(CH(CN)2)copper(I)

Guidance literature:: With P(C₆H₅)3; In dichloromethane; bubbling N2 through suspn.; evapn. to dryness; residue treated with Et2O;
DOI:10.1016/0022-328X(88)80403-0