bis(N,N-di(n-propyl)dithiocarbamato)dioxo(triphenylphosphine oxide)uranium(VI)

Base Information

• Chemical Name: bis(N,N-di(n-propyl)dithiocarbamato)dioxo(triphenylphosphine oxide)uranium(VI)
• CAS No.: 112614-53-6
• Molecular Formula: C₃₂H₄₃N₂O₃PS₄U
• Molecular Weight: 900.972
• Mol file: 112614-53-6.mol

Synonyms:

Chemical Property of bis(N,N-di(n-propyl)dithiocarbamato)dioxo(triphenylphosphine oxide)uranium(VI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(N,N-di(n-propyl)dithiocarbamato)dioxo(triphenylphosphine oxide)uranium(VI)

There total 1 articles about bis(N,N-di(n-propyl)dithiocarbamato)dioxo(triphenylphosphine oxide)uranium(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

uranyl nirate hexahydrate + N,N'-dipropyldithiocarbamate sodium (4143-50-4) + Triphenylphosphine oxide (791-28-6) → bis(N,N-di(n-propyl)dithiocarbamato)dioxo(triphenylphosphine oxide)uranium(VI) (112614-53-6)

Guidance literature:

In methanol; dimethyl sulfoxide; byproducts: sodium nitrate; a soln. of 1 equiv of UO2(NO3)2*6H2O in MeOH-DMSO was treated with 1 equiv of Ph3PO and 2 equiv of n-Pr2NCS2Na, stirred for 30 min at room. temp.; filtered, pptd. by adding H2O to the filtrate, filtered by suction, washed with H2O, dried over CaCl2 under vac., purified by dissolving in MeOH-DMSO and reprecipitating with H2O; elem. anal.;

DOI:10.1016/S0020-1693(00)84474-6

upstream raw materials:

N,N'-dipropyldithiocarbamate sodium

Triphenylphosphine oxide